382/2001 Sb.
The DECREE
Ministry of the environment
of 17 December. October 2001
on the conditions of application of the adapted sludge on agricultural land
Change: 504/2004 Sb.
The Ministry of environment in cooperation with the Ministry of
of agriculture and the Ministry of health provides under section 33, paragraph. 4
Act No. 185/2001 Coll., on waste and on amendments to certain other laws,
(hereinafter referred to as "the Act"):
PART THE FIRST
THE CONDITIONS OF APPLICATION OF THE ADAPTED SLUDGE ON AGRICULTURAL LAND
§ 1
The technical conditions for the application of the adapted sludge on agricultural land
Modified sludge ^ 1) can be used on agricultural land use under the following
terms and conditions:
and) no later than 48 hours from the location of the sludge on agricultural land must be
zapraveny sludges to soil;
(b)) the need to supply nutrients to the soil on the property to the location of the sludge must
be accompanied by the results of the analyses of agro-chemical properties of the soils referred to in
registration sheet the use of sludge in agriculture, according to annex No 1;
(c)) shall not use more than 5 tonnes of dry sludge per hectare during the
3 consecutive years. This amount may be increased up to 10
tonnes of dry sludge during 5 consecutive years, if used
sludges contain less than half the limit the quantity of each of the monitored
the risk of substances and elements. The exact determination of the benefits of dry matter shall be calculated from the
the observed nitrogen content. The dose of nitrogen supplied in sludge must not
exceed 70% of the total quantity of nitrogen needed for hnojenou
the crop. Batch sludge (the amount and duration of use) shall be governed by and request
plants for nutrients with regard to accessible nutrients and organic
folder in the soil, as well as to the various site conditions;
(d)) under the conditions provided for the levy of the sludge referred to in paragraph (c)) is on the
land applied in one agro-operation and in one contiguous
the time period for the favorable physical and humidity conditions;
e) minimum dry matter content of sludge for pressure incorporation
radlicovými applicators is 5%, minimum dry matter content of the sludge application
mechanical rozmetadly of organic fertilizers is 18%.
§ 2
The limit values for the concentration of selected high-risk substances in soil and
the risk of substances which may be added to the agricultural land
(1) in the soil, which can be used, not to be exceeded
the limit values for the concentration of selected risk substances listed in
Annex No 2.
(2) the total allowable risk vnos substances into agricultural land use
the Lees during 10 consecutive years is defined the allowable
dose the sludge referred to in article 1 (a). (c)) and the concentration limit values
the risk of substances and substances referred to in annex 3.
§ 3
The limit values for the concentration of selected risk substances and elements in sludge and
microbiological criteria for the use of sludge on agricultural land
On the agricultural land may only be used, that meet
and the limit values of concentration) of selected risk substances and elements
referred to in annex 3, and
(b)) the microbiological criteria set out in annex 4.
§ 4
The sampling procedures and methods of analysis of the soil and sludge and soil
(1) the sampling and analysis of samples of the soil (hereinafter referred to as the "monitoring of the land") on the
the grounds for the use of sludge and subscriptions, and analysis of samples of sludge (
"the monitoring of sludge") provide the originators of the sludge. The proposal for the monitoring of soil and
monitoring sludge on land intended for the use of the sludge is part of
program to use sludge on agricultural land under section 5.
(2) Monitoring of the soil is carried out before the first use of the sludge and
regular 10-year intervals in accordance with the particular legal
Regulation ^ 2), and in the scope specified in annexes 1 and 2.
(3) the monitoring shall be carried out when the sludge sampling and chemical and microbiological
analysis of sludge in the range and frequency as specified in annexes 3, 4 and 5.
For monitoring the Lees shall these requirements:
and determination of organic halogens) adsorbovatelných (AOX) and
polychlorinated biphenyls in sediments shall be carried out before the first use
sludge;
(b)) sampling of sludge is done according to the ČSN EN ISO 5667; ^ 3)
(c) samples of the sludge) for microbiological examination must be removed so that the
avoid secondary contamination, their preservation and transport shall be carried out
According to ČSN ISO 10381. ^ 4)
(4) Monitoring of the soil performs the person responsible for Central control and
test Institute agricultural under special legislation ^ 5)
the procedures laid down in the specific legislation. ^ 6)
(5) the reference methods for the analysis of samples of sludge and soils are listed in the
Annex No 6.
(6) the results of the monitoring of the sludge and soil monitoring stated on registration
the use of sludge in agriculture worksheet according to annex No 1, which is part of the
program using the sludge referred to in § 5. The annexes to the report are filled
always carried out the monitoring reports on the monitoring of soil and sludge. This
the originator of the sludge report archives for 30 years.
§ 5
The content of the programme, the use of sludge on agricultural land
(1) the use of sludge treated by the originator of the sludge always contains
and evaluation of sludge from the viewpoint of) their use on agricultural land in the
accordance with annexes 3, 4 and 5;
(b)) the enumeration of selected plots of land intended for the use of sludge, including indicators for the
their assessment according to annex No 2;
c) hydrological conditions in the area use of sludge;
(d) the inclusion of the use of sludge to) rotation;
(e) monitoring of the Lees and) the proposal for the monitoring of the soil;
(f) the sampling plan);
g) measures on health protection while working with sludges.
(2) part of the use of sludge are also accounting leaves the use of sludge
in agriculture, according to annex No 1.
PART THE SECOND
The EFFECTIVENESS of the
§ 6
This Decree shall take effect on 1 January 2005. January 1, 2002.
Minister:
RNDr. Kužvart in r.
Annex 1
Registration sheet of the use of sludge in agriculture
for the year ....
+-+-+-+-+-+
Registration number | | || ||
(Fill in the Municipal Office of | || || |
the municipality with the extended +-+-+-+-+-+
the competencies or
the urban part of the
HL. m. Prahy)
+-+-+-+
Sheet No. | | |1|
+-+-+-+
The number of sheets |
+-+-+-+
+-------------------------------------+-------------------------------------+
| The agent | A separate establishment |
+---------------------+-+-+-+-+-+-+-+-+---------------------+-+-+-+-+-+-+-+-+
| ID no.: | | |: Number | || || |
+---------------------+-+-+-+-+-+-+-+-+---------------------+-+-+-+-+-+-+-+-+
| Authorized person (name): | Name: |
| | |
| | |
+-------------------------------------+-------------------------------------+
| Street: | Street: |
+-------------------------------------+-------------------------------------+
| Location: | Location: |
+---------------------------+-+-+-+-+-+---------------------------+-+-+-+-+-+
| PSČ: | | | | | | PSČ: | | | | | |
+-------------------------+-+-+-+-+-+-+-------------------------+-+-+-+-+-+-+
| The Code Of The ODA (SOP) | The Code Of The ODA (SOP) |
+-------------------------+-+-+-+-+-+-+-------------------------+-+-+-+-+-+-+
| IC ZÚJ: | | | | | | | The person authorized to act on behalf of the company: |
| | | | | | | | |
+-------------------------+-+-+-+-+-+-+-------------------------------------+
| The date of the copy of the document:| | | | | | | Phone: |
| +-+-+-+-+-+-+-------------------------------------+
| Stamp and signature: | FAX: |
| +-------------------------------------+
| | The location of the wastewater treatment plant |
| +-------------------------------------+
| | The name of the village, the name of the village or: |
| | |
| +-------------------------+-+-+-+-+-+-+
| | ICZÚJ: | | | | | | |
+-------------------------------------+-------------------------+-+-+-+-+-+-+
| The owner of the wastewater treatment plant (ID, owner name, full address, the County Code (NUTS-4)) |
| |
| |
+---------------------------------------------------------------------------+
The user of sludge
+-------------------------------------+-------------------------------------+
| Holding or entitled | A separate establishment |
person (farmer) | | |
+---------------------+-+-+-+-+-+-+-+-+---------------------+-+-+-+-+-+-+-+-+
| CORPORATE ID | || || | the number of establishments: | | || ||
+---------------------+-+-+-+-+-+-+-+-+---------------------+-+-+-+-+-+-+-+-+
| Firm (name): | Name: |
| | |
| | |
+-------------------------------------+-------------------------------------+
| Street: | Street: |
+-------------------------------------+-------------------------------------+
| Location: | Location: |
+---------------------------+-+-+-+-+-+---------------------------+-+-+-+-+-+
| PSČ: | | | | | | PSČ: | | | | | |
+---------------------+-+-+-+-+-+-+-+-+-------------------------+-+-+-+-+-+-+
| IČ: | | | | | | | | | County Code (CZ-NUTS4): | |
+---------------------+-+-+-+-+-+-+-+-+-------------------------+-+-+-+-+-+-+
| County Code (CZ-NUTS4): | | IC ZÚJ: | | | | | | |
+-------------------------+-+-+-+-+-+-+-------------------------+-+-+-+-+-+-+
| IC ZÚJ: | | | | | | | The person authorized to act on behalf of the company: |
| | | | | | | | |
+-------------------------+-+-+-+-+-+-+-------------------------------------+
| OKEČ: | | | | | | Phone, FAX:
+-------------------------+-+-+-+-+-+-+-------------------------------------+
| The date of the copy of the document:| | | | | | | The total quantity of sludge: |
| +-+-+-+-+-+-+-------------------------------------+
| Stamp and signature: | Note: |
| | |
| | |
| | |
| | |
+-------------------------------------+-------------------------------------+
+-+-+
+-+-+-+-+-+-+-+-+-+-+ List č. | |2|
IČ +-+-+-+-+-+-+-+-+-+-+ +-+-+
The number of sheets |
+-+-+
Agrochemical soil properties of 1):
+----------------------+--------------------------+
| Soil reaction pH | |
+----------------------+--------------------------+
| Categories of land | |
+----------------------+--------------------------+
| The average content of in | mg. kg-1 |
| soil | |
+----------------------+--------------------------+
| Mg-magnesium | |
+----------------------+--------------------------+
| K-potassium | |
+----------------------+--------------------------+
| P-phosphorus | |
+----------------------+--------------------------+
+--------------+----------------+--------------------------------------+
| Risk element | Content in soil | The limit values for the concentration of elements in soil |
| | (mg.kg-1 dry weight) | (mg.kg-1 dry weight) |
| | +-------------------+------------------+
| | | Common land | Sands, loamy |
| | | | Sands, |
| | | | sand-gravel mix |
+--------------+----------------+-------------------+------------------+
| As-arsenic | | 20 | 15 |
+--------------+----------------+-------------------+------------------+
| CD-cadmium | | 0.5 | 0.4 |
+--------------+----------------+-------------------+------------------+
| CR-chromium | | 90.0 | 55.0 |
+--------------+----------------+-------------------+------------------+
| CU-copper | | 60.0 | 45.0 |
+--------------+----------------+-------------------+------------------+
| Hg-mercury | | 0.3 * | 0.3 * |
+--------------+----------------+-------------------+------------------+
| NI-nickel | | 50.0 | 45.0 |
+--------------+----------------+-------------------+------------------+
| PB-lead | | 60.0 | 55.0 |
+--------------+----------------+-------------------+------------------+
| Zn-zinc | | 120.0 | 105.0 |
+--------------+----------------+-------------------+------------------+
* the total content
2) supply of sewage sludge:
+---+---------------+------------+--------------------------------------------------+
|Č. | Date | Delivery | Hunt |
| | | Lees | |
+---+---------------+------------+--------------+--------------+---------+----------+
| | tonnes dry matter content | | % of dry matter for | Arch. microbiol. Hunt/| Size | The crop |
| | | | Hunt | coordinates | hunt | |
| | | | | | (ha) | |
+---+---------------+------------+--------------+--------------+---------+----------+
| | | | | | | |
+---+---------------+------------+--------------+--------------+---------+----------+
* coordinates according to the Bushmen in the results section 10 of the Act, AZP
No 156/1998 Coll.
+-+-+
+-+-+-+-+-+-+-+-+-+-+ List č. | |2|
IČ +-+-+-+-+-+-+-+-+-+-+ +-+-+
The number of sheets |
+-+-+
3) properties of sewage sludge
+--------------------+-----------------+---------------+-----------------+
| Sampling of:| | Protocol No. | |
+--------------------+-----------------+---------------+-----------------+
| Analysis of sludge of:| | Protocol No. | |
+--------------------+-----------------+---------------+-----------------+
| Analysis by: |
+------------------------------------------------------------------------+
| Number of attachments: |
+-------------------------------+-----------------------+----------------+
| The reference pointer | The content in the original matrix | The content in the dry matter |
| | (%) | (%) |
+-------------------------------+-----------------------+----------------+
|-organic substances loss on ignition | | |
+-------------------------------+-----------------------+----------------+
| N-total nitrogen | | |
+-------------------------------+-----------------------+----------------+
| NH4-N-ammonia | | |
+-------------------------------+-----------------------+----------------+
| NO3-N-nitric nitrogen | | |
+-------------------------------+-----------------------+----------------+
| CA-calcium | | |
+-------------------------------+-----------------------+----------------+
| Mg-magnesium | | |
+-------------------------------+-----------------------+----------------+
| K-potassium | | |
+-------------------------------+-----------------------+----------------+
| P-phosphorus | | |
+-------------------------------+-----------------------+----------------+
| The pH of the sewage sludge | | |
+-------------------------------+-----------------------+----------------+
+---------------------------+-------------+------------------+
| Reference | Secured | The limit |
| pointer | values | (maximum) |
| | (mg.kg-1) | values |
| | | concentration |
| | | in sludge |
| | | (mg.kg-1 |
| | | dry matter) |
+---------------------------+-------------+------------------+
| As-arsenic | | 30 |
+---------------------------+-------------+------------------+
| CD-cadmium | | 5 |
+---------------------------+-------------+------------------+
| CR-chromium | | 200 |
+---------------------------+-------------+------------------+
| CU-copper | | 500 |
+---------------------------+-------------+------------------+
| Hg-mercury | | 4 |
+---------------------------+-------------+------------------+
| NI-nickel | | 100 |
+---------------------------+-------------+------------------+
| PB-lead | | 200 |
+---------------------------+-------------+------------------+
| Zn-zinc | | 2500 |
+---------------------------+-------------+------------------+
| AOX | | 500 |
+---------------------------+-------------+------------------+
| PCBS (sum of congeners-6 | | 0.6 |
| 28 + 52 + 101 + 138 + 153 + 180) | | |
+---------------------------+-------------+------------------+
+-------------------------------------------------------+
| Vnos risk elements in the soil used dose of sludge |
| (kg ha-1) |
+------+------+------+------+------+------+------+------+
| Inc. | CD | CR | CU | Hg | NI | PB | Zn |
+------+------+------+------+------+------+------+------+
| | | | | | | | |
+------+------+------+------+------+------+------+------+
+-+-+
+-+-+-+-+-+-+-+-+-+-+ List č. | |3|
IČ +-+-+-+-+-+-+-+-+-+-+ +-+-+
The number of sheets |
+-+-+
+--------------------------+------------+-------------------------------------------+
| | Found | The permissible quantity |
| Micro-organism | values | micro-organisms (CFU *) in 1 g |
| | | the applied sludge dry matter |
| | +-------------------------------------------+
| | | Category of sludge |
| | +----------------------+--------------------+
| | (CFU) in 1 | I. | II. |
| | g dry matter | | |
| | Lees | | |
+--------------------------+------------+----------------------+--------------------+
| termotolerantní coliform | | < 10E3 | 10E3-10E6 |
| bacteria | | | |
+--------------------------+------------+----------------------+--------------------+
| enterococci | | < 10E3 | 10E3-10E6 |
+--------------------------+------------+----------------------+--------------------+
| Salmonella sp. | | the negative finding | does |
+--------------------------+------------+----------------------+--------------------+
* CFU-colony forming unit
1. the method of filling out a form provided in annex No 1 in the case of
the use of sludge from multiple vendors for each of the originator (the supplier)
fill separately in annex No. 1
Originator:
ID-identification number of organization to be completed (if any);
If your organization has less than eight-digit IDENTIFICATION NUMBER, make up zeros on the left
the total number of 8.
The originator or the beneficiary (name)-name of the agent or to be completed
authorized persons, as is registered in the commercial register or in
trades of the worksheet.
Street, place, POSTAL CODE-complete accurate and full address of the designer or
authorized person.
ODA (SOP) code is the code of the administrative area with extended
competence or administrative circuit hl. m. Prahy, in whose administrative territory
the headquarters of the originator or the beneficiary is located, according to the lists, which
they were introduced to the communication from the Czech Statistical Office, declared in the
The collection of laws under no. 471/2002 Sb.
ICZÚJ-is the identification number of the basic territorial unit, the place of the village
the address of the originator or the beneficiary. It is reported by the single
the dial of the municipalities of the CZECH REPUBLIC.
SIC code is the prevailing (main) economic activity by
The sectoral classification of economic activities released by the Czech Statistical
by the authority.
A separate place of business-means an establishment under section 5 (3). 1 of the law
No. 455/1991 Coll., on trades in the wording of later regulations.
The number of separate establishments which fills in the internal number of the establishment, if the
the originator or the beneficiary has the establishment numbered. In the opposite
If left blank, the competent District Office fills in the number in the
ascending order according to the order of an establishment registered for the District Office.
The name of the establishment-to be completed by the name of the establishment.
Street, place, POSTAL CODE-complete accurate and full address of the individual
of the establishment.
The code of the ODA (SOP) separate establishments-lists the code of the administrative circuit
municipalities with extended competence, or the administrative circuit hl. m. Prahy, on
the administrative territory of the headquarters of the originator, or the separate establishment
an authorized person is located, according to the lists, which were introduced by communication
The Czech Statistical Office, declared in the collection of laws under no.
471/2002 Sb.
The location of the establishment is identified by name and identification number of the
the basic territorial units of the municipality where the sludge is produced
The name of the village is the name of the village place of location of the plant.
ICZÚJ-is the identification number of the basic territorial units of the municipality, i.e.. space
the location of the establishment. It is reported by the single box of the municipalities of the CZECH REPUBLIC.
User:
ID-identification number of organization to be completed (if any):
If your organization has less than eight-digit IDENTIFICATION NUMBER, make up zeros on the left
the total number of 8. For the farmers, who do not have ID,
fills the birth number (if specified).
Firm (name)-name of the farm to be completed or authorized
persons, as is registered in the commercial register or in the trades
the worksheet.
Street, place, POSTAL CODE-complete accurate and full address of the designer or
authorized person.
ODA (SOP) code is the code of the administrative area with extended
competence or administrative circuit hl. m. Prahy, in whose administrative territory
the headquarters of the originator or the beneficiary is located, according to the lists, which
they were introduced to the communication from the Czech Statistical Office, declared in the
The collection of laws under no. 471/2002 Sb.
ICZÚJ-is the identification number of the basic territorial units of the village place
the address of the business. It is reported by the single box of the municipalities of the CZECH REPUBLIC.
SIC code is the prevailing (main) economic activity by
The sectoral classification of economic activities released by the Czech Statistical
by the authority.
A separate place of business-means an establishment under section 5 (3). 1 of the law
No. 455/1991 Coll., on trades, as amended
regulations. In the event that the company does not have a separate establishment, this right
the part is not used.
The number of separate establishments which fills in the internal number of the establishment, if the
the originator or the beneficiary has the establishment numbered. In the opposite
If left blank, the competent District Office fills in the number in the
ascending order according to the order of an establishment registered for the District Office.
The name of the establishment-to be completed by the name of the establishment.
Street, place, POSTAL CODE-complete accurate and full address of the individual
of the establishment.
The code of the ODA (SOP) separate establishments-lists the code of the administrative circuit
municipalities with extended competence, or the administrative circuit hl. m. Prahy, on
the administrative territory of the headquarters of the originator, or the separate establishment
an authorized person is located, according to the lists, which were introduced by communication
The Czech Statistical Office, declared in the collection of laws under no.
471/2002 Sb.
The number of agents of slurry (suppliers) on a plot of land-in the application of sludge at the
one of the plot from different suppliers (agents of sludge), the total
the number of suppliers.
Annex 2
The limit values for the concentration of selected elements in the soil (risk indicators
for the evaluation of soils)
+----------------------------------------------------------------+
| The limit values for the concentration of elements in the extract by Agua Royal |
| in the mg.kg-1 dry weight in soil |
+------------------+----+-----+-----+-----+-----+-----+-----+----+
| | Inc. | CD | CR | CU | Hg | NI | PB | Zn |
+------------------+----+-----+-----+-----+-----+-----+-----+----+
| Common land | 20 | 0.5 | 90 | 60 | 0.3 * | 50 | 60 | 120 |
+------------------+----+-----+-----+-----+-----+-----+-----+----+
| Sands, loamy | | | | | | | | |
| Sands, sand-gravel mix | 15 | 0.4 | 55 | 45 | 0.3 * | 45 | 55 | 105 |
+------------------+----+-----+-----+-----+-----+-----+-----+----+
* the total content
Explanatory notes:
1) limit values for concentrations of selected elements in the soil-defined
the maximum values of the selected risk elements in the soil, in the
the overrun could occur damage to the soil functions and components of the
environment
2) Categorization of soils:
and) Common (písčitohlinité, loamy clay), which occupy vast
part of the agriculturally used land. Under the terms of common land we understand soils
the normal variability of the element, with the normal soil development in the various
the geomorphologic conditions in areas of different psamitických,
pelitických rocks of sedimentary, acidic, neutral, and
basis of rocks of igneous and metamorphic rocks. It is therefore a
the land, which the cast of the geogenně and the petrograficky anomalous rocks,
such as sands, sand-gravel mix, ultrabazické rocks (hadce, amphibolites,
leucitity) and carbonate rocks. This includes the area where the
land involved in rock or veins with high degree of metalogenetického
minerals.
(b)), to very light, sandy and poor matečních rocks, such as
sand. In the case of the definition of these soils is required based on the
representation of fine particulate matter (10 microns), which consists of a maximum of 10
%. In soils of sandy on the sands, štěrkopíscích and štěrcích it is mainly in the
due to the low sorption ability, even in the case of direct use
raw materials with normal levels of risk elements leads to the rapid
pollution of the groundwater and river water.
(c)) and land on the substrates geogenně conditional extreme contents
some of the elements. These soils are evaluated separately and reference
the value of the background is not. For the soil on the other geogenně
the extreme upper limits are not these rocks of the reference values of the elements
determined, because their value in these rocks are often considerably
outstanding and high, especially for Cr, Co, Ni, and throughout the soil
profile.
Annex 3
The limit values for the concentration of selected risk substances and elements for sewage sludge.
their use on agricultural land (indicators for the evaluation of sludge)
+------------------------+---------------------------+
| Risk substance | The limit (maximum) value |
| | concentrations in sludge |
| | (mg.kg-1 dry weight) |
+------------------------+---------------------------+
| As-arsenic | 30 |
+------------------------+---------------------------+
| CD-cadmium | 5 |
+------------------------+---------------------------+
| CR-chromium | 200 |
+------------------------+---------------------------+
| CU-copper | 500 |
+------------------------+---------------------------+
| Hg-mercury | 4 |
+------------------------+---------------------------+
| NI-nickel | 100 |
+------------------------+---------------------------+
| PB-lead | 200 |
+------------------------+---------------------------+
| Zn-zinc | 2500 |
+------------------------+---------------------------+
| AOX | 500 |
+------------------------+---------------------------+
| PCBS (sum of congeners-6 | |
| 28 + 52 + 101 + 138 + 153 + 180) | 0,6 |
+------------------------+---------------------------+
Annex 4
Microbiological criteria for the use of sludge on agricultural land
+--------------+-----------------------------------------------+
| | The permissible amount of micro-organisms (CFU *) |
| Category of sludge | in 1 gram of dry sludge applied |
| +--------------------+-----------+--------------+
| | termotolerantní | enterococci | Salmonella sp. |
| | coliform bacteria | | |
+--------------+--------------------+-----------+--------------+
| I. | < 10E3 | < 10E3 | negative |
| | | | find |
+--------------+--------------------+-----------+--------------+
| II. | 10E3-10E6 | 10E3-10E6 | does |
| | | | with |
+--------------+--------------------+-----------+--------------+
* CFU-colony forming unit
Explanatory notes:
Category I-sludge, which can be generally applied to land used in the
Agriculture in compliance with the other provisions of this Ordinance.
Category II-sludge, which can be applied to agricultural land
for the cultivation of industrial crops, and on the land, on which at least 3 years
After the application of sewage sludge will not grow vegetables and field
intensely fruit-bearing fruit planting, and in compliance with the principles of the protection of the health
at work and other provisions of the Ordinance.
Annex 5
The minimum frequency of chemical and microbiological analyses of sludge
used on agricultural land per year
+-----------+------------------------------------------------------------------+
| | The minimum number of analyses for the year |
| +-------------+-------------------+------------------+-------------+
| Production | agrochemical | the risk elements | Microbiology | organic |
|-sludge | parameters | (As, Cd, Cr, Cu, | (termotoler, environmental contaminants |
| WASTEWATER TREATMENT PLANT | (nutrients) | Hg, Ni, Pb, Zn) | kaliform. | (AOX, PCB) |
| (in tonnes | | | bacteria | |
the dry sludge | | | | enterococci, | |
|/year) | | | Salmonella sp.) | |
+-----------+-------------+-------------------+------------------+-------------+
| | | | | ** |
| < 250 | 2 | 2 | 2 | - |
+-----------+-------------+-------------------+------------------+-------------+
| 250-1000 | 4 | 4 | 4 | ** |
| | | | | - |
+-----------+-------------+-------------------+------------------+-------------+
| 1000-2500 | 4 | 4 | 6 | 1 |
+-----------+-------------+-------------------+------------------+-------------+
| > 2500 | 12 | 12 | 12 | 1 |
+-----------+-------------+-------------------+------------------+-------------+
* agrochemical parameters: pH, solid content, the content of the organic
substances (expressed as the loss on ignition)
total nitrogen, ammonia nitrogen,
nitric nitrogen, phosphorus, potassium,
calcium, magnesium
the analysis are made according to the section 4, paragraph 4. 2 this order before the
the first use of sludge
Annex 6
Methods of sampling, analysis and methods for microbiological determination
+----------------------------------+-----------------------------+
| The subject matter, the purpose of the | standard |
| pointer | |
+----------------------------------+-----------------------------+
| Guidelines for the sampling of sludges ČSN EN ISO 5667 sampling |
from sewage plants and treatment plants, | | part 13 |
+----------------------------------+-----------------------------+
| Soil quality-sampling-| ČSN ISO 10 381-6 |
Part 6: Instructions for subscription | |
handling and storage | | |
the soil samples intended for ' | ' | |
the study of aerobic microbial | | |
processes in the laboratory, | | |
+----------------------------------+-----------------------------+
| The quality of the soil-sample preparation | ČSN ISO 11 464 |
' | ' for physico-chemical analysis | |
+----------------------------------+-----------------------------+
| Physico-chemical analysis of sludge | CSN 83 05 50 part 3 |
|-Determination of total dry matter | |
After annealing and the rest of the ' | ' loss | |
| ignition | |
+----------------------------------+-----------------------------+
| Physico-chemical analysis of sludge-| ČSN EN 12 176 |
| Determination of pH | |
+----------------------------------+-----------------------------+
| Soil quality-determination of pH | ČSN ISO 10 390 |
+----------------------------------+-----------------------------+
| Soil quality-determination of total | ČSN ISO 11 261 |
|-nitrogen modified | |
| Kjeldahl method | |
+----------------------------------+-----------------------------+
| Soil quality-determination of | ČSN ISO 11 465 |
percentage by weight of dry matter and | | |
|-soil moisture by weight | |
| Gravimetric method | |
+----------------------------------+-----------------------------+
| Characterization of sludges-| EN 13346 |
| Determination of trace elements | |
|-Aqua regia and phosphorus | |
extraction methods | | |
| | |
| Characterization of sludge. Design of CSN EN determination | 13346 |
trace elements and phosphorus |. | |
| Method of extract by Agua | |
| Royal | |
+----------------------------------+-----------------------------+
| Determination of 33 elements by Atomic | ČSN EN ISO 11 885 |
emission spectrometry with | | |
Inductively bound plasma | | |
| (P, K, Na, Ca, Mg, Cd, Cr, Cu, Ni, Pb, Zn) | |
+----------------------------------+-----------------------------+
| The quality of the water. The determination of all to CSN 75 74 40 TNV | |
Mercury Atomic dedicated | | |
| Absorption Spectrometer | |
+----------------------------------+-----------------------------+
| The quality of the water. Determination of mercury | EN 1483 |
+----------------------------------+-----------------------------+
| Soil quality-Extraction of | ISO 11 466 |
trace elements soluble in ' | ' | |
aqua regia | (As, Cd, Cr, Cu, Ni, Pb, | |
| Zn) | |
+----------------------------------+-----------------------------+
| The quality of the water. Determination of sodium 1 | ISO 9964-1,2,3 (75 7378) |
|, and potassium. Part 1-3: determination | |
' | ' sodium and potassium Atomic method | |
| absorption spectrometry | |
+----------------------------------+-----------------------------+
| The quality of the water. Determination of calcium 1 | ISO 7980 (75 7383) |
|, and magnesium. Method of Atomic | |
| absorption spectrometry | |
+----------------------------------+-----------------------------+
| The quality of the water. Determination of Co, Cu, Ni, ČSN ISO 8288 |
| Zn, Cd and Pb methods of flame | |
| atomic absorption spectrometry | |
+----------------------------------+-----------------------------+
| The quality of the water. Determination of Cr method | EN 1233 |
| atomic absorption spectrometry | |
+----------------------------------+-----------------------------+
| The quality of the water. Determination of Cd Atomic | ČSN EN ISO 5961 |
| absorption spectrometry | |
+----------------------------------+-----------------------------+
| Schlamm und Sedimente. Bestimmung | DIN 38414-18 |
| von adsorbierten organisch | |
| gebundenen halogenen (AOX) | |
+----------------------------------+-----------------------------+
| Schlamm und Sedimente. Bestimmung | DIN 38414-20 |
| polychlorierten biphenylen von 6 | |
| (PCB) | |
+----------------------------------+-----------------------------+
| General instructions for preparing | 6887 ČSN ISO |
dilution in microbiological | | |
| testing | |
+----------------------------------+-----------------------------+
| General guidelines for ' ISO 7218 |
Microbiological testing | | |
+----------------------------------+-----------------------------+
| The quality of the water. General guidelines for ' ISO 8199 |
determination of micro-organisms | | |
| cultivation | |
+----------------------------------+-----------------------------+
| The recommended method for determining | ČSN EN 12 824 |
detection of bacteria of the genus Salmonella | | |
| sp. in sludge from WASTEWATER TREATMENT PLANT | |
+----------------------------------+-----------------------------+
| The recommended method for fixing | The modified ISO 7899-2 |
| termotolerantních counts | |
coliforms in sewage sludge, | | |
|z ČOV* | |
+----------------------------------+-----------------------------+
| The recommended method for fixing | The modified ISO 9308-1 |
| termotolerantních coliform | |
|: Microbiology. | |
| General guidelines for the determination of | |
| the number of coliforms. | |
| The technique of counting kolinií * | |
+----------------------------------+-----------------------------+
the procedures are published in the Acta microbiologica hygienica and (AHEM)
No. 7/2001.
section 32 (a)) 1. (b)) Law No 185/2001 Coll., on waste and amending certain
other laws.
2) § 2 (2). 1 (a). and), b), c) Decree No. 275/1998 Coll., on
agrochemickém testing of agricultural soils and soil properties of discovery
forest land, as amended by Decree No. 477/2000 Sb.
3) EN ISO 5667-13: guidance on sampling of sludges from sewage plants and
water treatment plants.
4) ISO 10381-6: soil quality-sampling-part 6: guidelines for
collection, handling and storage of soil samples intended for the study of
aerobic microbial processes in the laboratory.
5) section 10 (1). 2 Act No. 156/1998 Coll., on fertilisers, supporting soil
substances, preparations and auxiliary plant substrates and
agrochemickém testing of agricultural soil (fertilizers Act), as amended by
amended.
6) Decree No 275/1998 Coll., as amended by Decree No. 477/2000 Sb.
