On Technical Requirements For Production, Storage And Processing Of Alcohol

Original Language Title: o technických požadavcích na výrobu, skladování a zpracování lihu

Read the untranslated law here: https://portal.gov.cz/app/zakony/download?idBiblio=45384&nr=141~2F1997~20Sb.&ft=txt

141/1997 Sb.



DECREE



The Ministry of agriculture



of 20 December. June 1997



on technical requirements for production, storage and processing of alcohol



82/2000: Sb.



Change: 82/2000 Coll. (part)



386/2003: Sb.



Change: 386/2003 Coll. (part)



88/2007: Sb.



190/2008: Sb.



The Ministry of agriculture, in agreement with the Ministry of industry and trade

determined in accordance with § 21 para. 1 of the law No. 61/1997 Coll., on alcohol and about the change and

additions to law No. 455/1991 Coll., on trades

(Trade Act), as amended, and the Act of the Czech

the National Council No. 587/1992 Coll. on the Excise Tax Act, as amended

legislation (the law on alcohol):



§ 1



Technical requirements for production facilities of the distilleries and their arrangement



(section 5 of the law on alcohol)



(1) this Ordinance has been notified in accordance with the directive of the European

Parliament and Council Directive 98/34/EC of 22 December 2004. June 1998 on the procedure for

the provision of information in the field of technical standards and regulations and of rules

for information society services, as amended by Directive 98/48/EC.



(2) a production facility of the distillery are devices, pipes, and areas in the

which is ethyl alcohol and spirituous couples unregistered control spirit meter

(hereinafter referred to as "the meter"), as well as a device to collect water, and lutrových

separated oils and waxes, and lutrovými waters shall mean waters

resulting from the acquisition of ethyl alcohol in the manner prescribed by law, and that after

distillation Department.



(3) production equipment of the distillery is produced of metal or other material

resistant to the action of alcohol, alcoholic vapours, operating temperatures and pressures.



(4) it is used only for soldering brazing. To seal is used only

materials resistant to change and effect of temperatures and pressures and exposure to alcohol and

alcoholic vapours.



(5) the pipeline, which is headed by ethyl alcohol and spirituous couples must not be damaged or

repaired.



(6) production equipment Coatings do not cover song distillery

the material from which the appliance is made. The pipeline, through which

ethyl alcohol and spirituous is kept in pairs, the walls or the ceiling, leaving around this

the pipeline space to explore. This space shall be covered

amended the relevant technical standard ^ 1).



(7) the pipes connecting the cooler with the meter must have:



and momentum)



(b)) the internal diameter of the corresponding performance of the distillation apparatus,



c) capping on all connections (flanges, valves, šroubeních

etc.).



(8) pursuant to paragraph 7 (b). (c)) may be made of an unpainted

galvanized sheet metal or other material relevant properties

agreed by the tax administrator ^ 1a) and must be adapted to the application

conclusions.



(9) on the connecting pipe of the cooler is placed with the measuring instrument epruvety,

sampling taps, vent equipment, quantity regulators

odtékajícího intrusion prevention device and steam and mash into the

the gauge.



(10) returns to the return flow of the heating boiler of the distillation of alcohol

the device must



and the supply pipe of mash feed) into a special metal containers mounted

at the bottom of the heating boiler distillation apparatus so that this vessel will remain

filled with záparou even after emptying the heating boilers and penstocks will

completely immersed in the leftover mash,



(b)) to be the drain pipe výpalkové tuned to the heating boiler

distillation apparatus left over at least the amount of the corresponding shapes

10% of the volume of the heating boiler.



(11) in the distillery, chemical, where it is used in the production of circulating

(gastroesophageal reflux) reservoir, the flow of the synthetic destilačně of ethyl alcohol of

This reservoir shall be adjusted so that when the recovery of alcohol from this tank



and in the pipeline for synthetic) technical alcohol ethyl alcohol was created with minimal

the content of higher alcohols and volatile substances designated for synthetic

technical ethyl alcohol,



(b) the sewage tank was) alcohol devalued by mixing the raw material for

the production of synthetic technical alcohol.



(12) the region of Distillery, where he presented dokapy to device

for collecting the lutrových waters, with a mixture of spills and dokapů with water lutrovými

considered to lutrové water.



§ 1a



Technical requirements for the equipment for continuous denaturing



[to section 21 (1) (a)), and (c)) of the ethyl alcohol]



(1) supply pipe, which is guided by a denaturant in the

continuous denaturing shall be before the mouth of the pipe leading alcohol

fitted with a meter.



(2) the amount of resource used in the continuous endorsement

denaturing alcohol is measured by gauges conforming to the requirements of the law on

Metrology ^ 1b).



§ 2



Technical requirements for the equipment for storage of alcohol



(section 14 of the law on alcohol)



(1) Equipment for the storage of alcohol are tanks, barrels, shipping containers

or containers that meet the requirements laid down by the law on metrology ^ 1b),

in which it is stored and transported by the spirit.



(2) facilities for the storage of alcohol is made from a material resistant to

the action of the spirit.



(3) the tank shall affix the volume.



(4) the fuel tank is filled up to 95 percent of volume.



(5) the fitting on the bottom of the tank is made of steel or brass.

The tank shall be at least 600 manhole diameter mm. Venting the

connects at the top part of the tank and adjusts so that it get too comfortable

ethyl alcohol or water.



(6) the tank higher than 2 m must be fitted with a device allowing

the taking of samples in each quarter of the height of the hole in the lid or adapted

to run the sample device allowing the sampling of

different layers.



§ 3



Methods of determining the volume of a volumetric concentration of ethyl alcohol and

How to calculate the amount of alcohol



[to section 21 (1) (b)) of the law on alcohol]



(1) For determination of the volumetric concentration and the volume of alcohol,

the exception of ethyl alcohol denatured, of the results of the measurements



and the density of the set pyknometrickou method),



(b)) with a hydrometer, which laid down the density satisfies the conditions laid down

the law on metrology ^ 1b) for measurements at a temperature of 20 degrees C,



(c)) method gas chromatography,



d) density laid down by means of electronic frequency oscillator,

or



e) density laid down using a hydrostatic balance.



In the case of denatured ethyl alcohol shall follow the procedure referred to in paragraph 8

.



(2) by volume of ethyl alcohol in the přiboudlině shall be pyknometrickou

method in the distillate from a water solution obtained by extraction of fusel oil

with light petroleum for the addition of a saturated solution of sodium chloride or

the method of gas chromatography.



(3) the Density of ethyl alcohol shall be calculated according to the formula given, including

factors in annex 1, part A.



(4) in determining the volume of ethyl alcohol, where the volume of ethyl alcohol is measured in

storage tanks of steel or in gauges of steel or britania

stipulated by special legislation ^ 2), the correction is carried out

thermal volume expansion of these materials by multiplying the observed

alcohol volume correction factor referred to in annex 1, part b.



(5) in determining the volumetric concentration of ethyl alcohol pyknometrickou method

performs correction for thermal dimensional expansion pycnometers of various

types of glass by multiplying the observed density correction factor referred to in

Annex 1, section C.



(6) the calculation of the volume of ethanol is carried out in the manner specified in the

Annex No 1 of part (D).



(7) when using multiple methods of measurement referred to in paragraph 1 is crucial

the result of the measurements carried out by the method of determining the density determined by pycnometry.



(8) For the determination of the mass concentration of denatured alcohol are

the applicable measurement results



and gas chromatography) method, or



(b)) by liquid chromatography.



(9) when using multiple methods of measurement referred to in paragraph 8 is crucial

the result of the measurements carried out by the method of gas chromatography.



§ 4



Types of denaturants and their minimum quantity and purpose of the

use denatured alcohol



(section 10 of the law on alcohol)



Types of denaturants, their minimum quantity and purpose of the

use denatured alcohol are listed in annex 2.



§ 5



Breakdown of the basic types of alcohol and their qualitative characters



(section 11 of the law on alcohol)



(1) for a more detailed breakdown of the basic types of spirit and quality characters

individual types of alcohol are listed in annex 3.



(2) an oddly denatured and denatured ethyl alcohol must comply with the

physical and chemical requirements for the respective type of alcohol and must

correspond to the valid technical standards.



§ 6



Methods for the determination of qualitative characters



(section 11 of the law on alcohol)



(1) the content of methanol is determined by gas chromatography.



(2) the content of higher alcohols is determined by gas chromatography

and is expressed as the sum of the recorded contents of each higher

alcohols.



(3) the content of aldehydes is determined colorimetrically using

fuchsinsiřičitého reagent and is evaluated as the contents of acetaldehyde or

the method of gas chromatography and is expressed as the sum of identified

the contents of the various aldehydes.



(4) the content of furalu is determined by colorimetry method or gas

chromatography.



(5) the content of the free acids, whose total content is evaluated as

the acetic acid content is determined by titration of the sample of the alcohol is free of carbon

dioxide concentration of sodium hydroxide solution 0.1 mol/l,


where appropriate, the method of gas chromatography.



(6) the contents of nitrogenous bases, the content of which is treated as content

metylaminu, is determined by titration of the sample solution of sulphuric acid on the

the concentration of 0.005 mol/l indicator according to Maa-Zuazagy or

bromkresolovou foliage or by gas chromatography.



(7) the content of odparku is determined from the sample with a volume of 250 ml with ethyl alcohol

the fermentation of the finest non-denatured, or about the volume of 100 ml

for other types of non-denatured ethyl alcohol. After evaporation and drying of the sample

at a temperature of 103 degrees (C) up to 107 degrees C, and after cooling in the

desiccator dried the rest of the sample, weighed on analytical scales.



(8) the content of esters is determined by titration of the sample of ethyl hydroxide solution

sodium 0.1 mol/l indicator by Simpson and

is evaluated as etylnatého acetate content or method of gas

chromatography and is expressed as the sum of the recorded contents

each of the esters.



(9) dietyléteru and benzene Content shall be determined by the method of gas

chromatography.



(10) the total content of higher alcohols and other volatile constituents of ethyl alcohol

synthetic technical is determined by gas chromatography.



(11) a content in volatile denaturants in denatured alcohol is

determined by gas chromatography.



(12) the resolution of the alcohol fermentation and alcohol synthetic izotopovými is carried out

methods.



(13) the content of Denatonium benzoate (Benzyldiethyl-N-2.6-xylyl-

-carbamoyl methyl ammonium benzoate) is determined by a combination of gas

chromatography with mass spectrometry or a method combination

high-performance liquid chromatography with mass spectrometry.



(14) the content of 2-methyl-2-propanol by gas

chromatography.



§ 7



Alcohol loss standards



[to section 21 (1) (b), (e)) of the ethyl alcohol]



The basis for the calculation of the individual types of alcohol loss and their standards above

are set out in annex 4.



§ 8



The loss of transport



[to section 2, paragraph 1, point (a). to) of the ethyl alcohol]



(1) the loss of transport shall be determined as the difference between sent and received

the quantity of alcohol. Transport losses include losses arising



natural evaporation of alcohol) during transport,



(b)) as a result of the permissible differences in measuring the amount of alcohol before sending and

After the adoption of the alcohol.



(2) the loss of transport do not apply to the quantity of alcohol contained in the

of finished products made from ethyl alcohol.



(3) the Pumping loss standards shall be assessed for each individual package

separately. In the basis for calculation of standard losses cannot be included

the quantity of alcohol in those packages for which has not been detected or loss

which have been found exceeding the standard loss loss.



§ 9



Loss handling



[to section 2, paragraph 1, point (a). to) of the ethyl alcohol]



Loss of handling are losses of alcohol resulting from the receipt and issue of

ethyl alcohol and other technologically necessary handling of alcohol (transfer of

ethyl alcohol in the manufacturers of alcohol). These losses include loss of

arising from the transfer of alcohol prior to transport alcohol in cases where alcohol

alcohol cannot be picked directly from the warehouse to the shipping containers and pits and

alcohol must be přečerpáván first.



§ 10



The loss of storage



[to section 2, paragraph 1, point (a). to) of the ethyl alcohol]



Storage losses are decreases of ethyl alcohol in stores, which arise

by evaporation during storage.



§ 11



The loss of the bottling



[to section 2, paragraph 1, point (a). to) of the ethyl alcohol]



Loss of bottling is calculated as the difference between the quantity of alcohol contained in the

product to bottling and the quantity of alcohol contained in the finished

the product passed on uk processors of ethyl alcohol in consumer packaging.



§ 12



Losses when modifying alcohol



[to section 2, paragraph 1, point (a). to) of the ethyl alcohol]



(1) the loss of refining is calculated as the difference between the quantity of raw

alcohol used for refining and the quantity of alcohol contained in a refined

alcohol and úkapech, dokapech and přiboudlinách.



(2) loss of dehydration is defined as the difference between the quantity of alcohol

used for the dehydration and the quantity of alcohol contained in the manufactured

water-free alcohol and other by-products containing dehydration

alcohol.



(3) the loss of the rectification shall be determined as the difference between the quantity of alcohol

contained in spirits intended for rectification and the quantity of alcohol

contained in rektifikovaném of the distillate and in úkapech and dokapech.



(4) loss of regeneration is determined as the difference between the amount of alcohol

contained in fabrics from which the alcohol is to be obtained, and the quantities again

obtained with the three spirits.



section 13 of the



Losses of alcohol



[to section 2, paragraph 1, point (a). to) of the ethyl alcohol]



The loss of alcohol during the processing of ethyl alcohol shall be determined as the difference between the amount of

ethyl alcohol used in the manufacture and the quantity of alcohol contained in stock or in the

the finished product.



§ 14



Transitional provision



The calculation of the loss standards of alcohol shall be carried out according to existing regulations



and industrial distilleries), distilleries, carrying out specific

refining or refinement of ethyl alcohol in the spirits and manage the material reserves

30. September 1997,



(b)) in the agricultural distilleries, and fruit to the date of termination of the seasonal production

and when the continuous production then to 30. September 1997,



c) distilleries and special distilleries not referred to in letters a and b))

and for the producers of spirits and other alcohol, including vinegar into processors 31.

December 1997,



(d)) in the distilleries, which are also the producers of spirits, to the date of their

seasonal production of ethyl alcohol and alcohol production to continuous 30. September 1997.



§ 15



The effectiveness of the



This Decree shall enter into force on 1 January 2000. July 1997.



Minister:



Ing. Lux in r.



Annex 1



PART AND



THE FORMULA FOR CALCULATING DENSITY

12 k-1 6 to

ro = sum A1 + and p + sum B (t-20 ° c) +

k = 2 k = 1 k



n I i

+ sum sum of C p (t-20 ° c).

I = 1 k = 1 i, k



n = 5

M1 = 11

M2 = 10

M3 = 9

M4 = 4

M5 = 2



The value of the coefficients:



k Ak Bk

kg/m3



1 012 300 9.982. 102-2.061 851 3. 10-1 kg/(m3. ° c)

2-1.929 769 495. 102-5.268 254 2. 10-3 kg/(m3. ° c 2)

3 238 958 3.891. 102 3.613 001 3. 10-5 kg/(m3. ° c 3)

4-103 923 1.668. 103-3.895 770 2. 10-7 kg/(m3. ° c 4)

5 1.352 215 441. 104 7.169 354 0. 10-9 kg/(m3.5 ° c)

6-278 388 8.829. 104-9.973 923 1. 10-11 kg/(m3. ° c 6)

7 874 042 3.062. 105

8-381 234 6.138. 105

9 7.470 172 998. 105

10-5.478 461 354. 105

11 2.234 460 334. 105

12-3.903 285 426. 104



C1, C2, to the

kg/(m3. ° c) kg/(m3. ° c 2)



1 443 461 530 087 1.693. 10-1-013 005 057 010 1.193. 10-2

2-914 743 455 169 1.046. 101 2.517 399 633 803 461. 10-1

3 353 469 546 523 7.196. 101-2.170 575 700 536 993

4-7.047 478 054 272 792. 102 034 988 843 029 1.353. 101

5 090 430 035 045 3.924. 103-5.029 988 758 547 014. 101

6-164 659 068 747 1.210. 104 1.096 355 666 577 570. 102

7 of 2.248 646 550 400 788. 104-1.422 753 946 421 155. 102

8-562 982 188 164 2.605. 104 1.080 435 942 856 230. 102

9 1.852 373 922 069 467-104-153 236 817 392 4.414. 101

10-7.420 201 433 430 137. 103 7.442 971 530 188 783

11 1.285 617 841 998 974. 103



to C3, C4, kC5, to

kg/(m3. ° c 3) kg/(m3. ° c 4) kg/(m3.5 ° c)



1-995 733 503 6.802 803.10-4 027.10-6 376 675 622 4.075-2.788 409.10 074354 782-8

2 837 790 289 664.10 1.876-2-8.763 058 573 471 110.10-6 612883 493 1.345 354.10-8

3-561 813 734 156.10 2.002-1 031 360 099 6.515 368.10-6

4 1.022 992 966 719 220-1.515 784 836 987 210.10-6

5-2.895 696 483 903 638

6 4.810 060 584 300 675

7-4.672 147 440 794 683

8 2.458 043 105 903 461

9-5.411 812.10 227 621 436-1



Note:



1. This formula applies to the measurements carried out at temperatures between

-20 ° c to + 40 ° c.



2. The values derived from this formula is calculated in the official

alcohol tables (part 1-3), issued by the

The Ministry of Agriculture of the CZECH REPUBLIC, Prague, 1995.



PART (B)



Table of values of the correction factors (Fb) to perform the correction on the

thermal volume expansion material at temperature t (in ° c-1)

material: steel



The temperature coefficient of volumetric expansion coefficient (beta) = 36. 10-6

C-1



t Fb t Fb



-20 0.99856 10 0.99964

-19 0.99860 11 0.99968

-18 0.99863 12 0.99971

-17 0.99867 13 0.99975

-16 0.99870 14 0.99978

-15 0.99874 15 0.99982

-14 0.99878 16 0.99986

-13 0.99881 17 0.99989

-12 0.99885 18 0.99993

-11 0.99888 19 0.99996

-10 0.99892 20 1.00000

-9 0.99896 9 1.00004

-8 0.99899 22 1.00007

-7 0.99903 23 1.00011

-6 0.99906 24 1.00014

-5 0.99910 25 1.00018

-4 0.99914 26 1.00022

-3 0.99917 27 1.00025

-2 0.99921 28 1.00029

-1 0.99924 29 1.00032

0 0.99928 30 1.00036

1 0.99932 31 1.00040

2 0.99935 32 1.00043

3 0.99939 33 1.00047

4 0.99942 34 1.00050

5 0.99946 35 1.00054

6 0.99950 36 1.00058

7 0.99953 37 1.00061

8 0.99957 38 1.00065

9 0.99960 39 1.00068

10 0.99964 40 1.00072



Material: Britanium



The temperature coefficient of volumetric expansion coefficient (beta) = 61. 10-6

C-1



t Fb t Fb



0 0.99878 20 1.00000

1 0.99884 21 1.00006

2 0.99890 22 1.00012


3 0.99896 23 1.00018

4 0.99902 24 1.00024

5 0.99909 25 1.00031

6 0.99915 26 1.00037

7 0.99921 27 1.00043

8 0.99927 28 1.00049

9 0.99933 29 1.00055

10 0.99939 30 1.00061

11 0.99945 31 1.00067

12 0.99951 32 1.00073

13 0.99957 33 1.00079

14 0.99963 34 1.00085

15 0.99970 35 1.00092

16 0.99976 36 1.00098

17 0.99982 37 1.00104

18 0.99988 38 1.00110

19 0.99994 39 1.00116

20 1.00000 40 1.00122



PART (C)



Table of values of the correction factors (Fb) to perform the correction on the

thermal volume expansion pycnometers of various types of glass in

temperature t (in ° C-1)



The temperature coefficient of volumetric expansion coefficient (beta) column:



a) = 5. 10-6 ° c-1



(b)) = 10. 10-6 ° c-1



(c)) = 15. 10-6 ° c-1



(d)) = 20. 10-6 ° c-1



(e)) = 25. 10-6 ° c-1



(f)) = 30. 10-6 ° c-1



g) glass normal quartz = 1.6. 10-6 ° c-1



h) normal Simax glass = 8.8. 10-6 ° c-1



I) glass normal Sial = 13.0. 10-6 ° c-1



j) glass normal Neutral = 17.0. 10-6 ° c-1



k) glass normal DC = 24.0. 10-6 ° c-1



l) glass normal Unihost = 27.0. 10-6 ° c-1

t/a column



a) b) c) d) e) f)



15 1.000025 1.000050 1.000075 1.000100 1.000125 1.000150

16 1.000020 1.000040 1.000060 1.000080 1.000100 1.000120

17 1.000015 1.000030 1.000045 1.000060 1.000075 1.000090

18 1.000010 1.000020 1.000030 1.000040 1.000050 1.000060

19 1.000005 1.000010 1.000015 1.000020 1.000025 1.000030

20 1.000000 1.000000 1.000000 1.000000 1.000000 1.000000

21 0.999995 0.999990 0.999985 0.999980 0.999975 0.999970

22 0.999990 0.999980 0.999970 0.999960 0.999950 0.999940

23 0.999985 0.999970 0.999955 0.999940 0.999925 0.999910

24 0.999980 0.999960 0.999940 0.999950 0.999900 0.999880

25 0.999975 0.999950 0.999924 0.999900 0.999875 0.999850



g) h) i) j) k) l)



15 1.000008 1.000044 1.000065 1.000087 1.000122 1.000135

16 1.000006 1.000035 1.000052 1.000070 1.000097 1.000108

17 1.000005 1.000026 1.000039 1.000052 1.000073 1.000081

18 1.000003 1.000018 1.000026 1.000035 1.000049 1.000054

19 1.000002 1.000009 1.000013 1.000017 1.000024 1.000027

20 1.000000 1.000000 1.000000 1.000000 1.000000 1.000000

21 0.999998 0.999991 0.999987 0.999983 0.999976 0.999973

22 0.999997 0.999982 0.999974 0.999965 0.999951 0.999946

23 0.999995 0.999974 0.999961 0.999948 0.999927 0.999919

24 0.999994 0.999965 0.999948 0.999930 0.999903 0.999892

25 0.999992 0.999956 0.999935 0.999913 0.999879 0.999865



PART (D)



How to calculate the volume of ethanol

and the calculation of the volume of ethanol) in the (unit: m3 or

L = dm3) for weighing solution of ethanol and water shall be carried out according to the

formula:



IN = OUT. km



where is the volume of ethanol at 20 degrees C in litres



From the apparent weight of the solution of ethanol and water as recorded by weighing

on the air (unit: kg)



km is a conversion factor (unit: dm3/kg = L/kg), which is

calculated according to the formula:



10 1 1

km = deltaE.----. [1 + roa ( ----- - ---- )]

ro20 ro20 roZ



where deltaE is volume concentration of ethanol in solution of ethanol and water

(unit:% = 0.01)



ro20 is the density of solution at a temperature of 20 degrees C (unit: kg/m3)



ROA is the air density (unit: kg/m3, the value:

1.2 kg/m3)



Roz is the density of the weight (unit: kg/m3, the value:

8 000 kg/m3)



(b)) the calculation of volume of ethanol in (unit: m3 or

L = dm3) when measuring the volume of solution of ethanol and water volume meter

at temperatures from-20 ° c to + 40 ° c shall be carried out according to the

formula:



In = in 't. FB. kV



where is the volume of ethanol in litres

In 't is the apparent volume of the reading on the gauge of the volume at a temperature

measurement in t (unit: m3 or L = dm3

FB is the correction factor for the gauge of volume thermal expansion

(unit: 1)

kV is a conversion factor (unit: 1), which is calculated

According to the formula:



Delta ro

E t

kv = ------ . ----

100 ro

20



where delta is by volume of ethanol in solution of ethanol and water

E (unit:% = 0.01)



ro is the density of the solution of ethanol and water at temperature t (unit:

t kg/m3)



ro is the density of the solution of ethanol and water at a temperature of 20 ° C

20 (unit: kg/m3)



Note:

Values of the coefficients are calculated by the formulas are listed

in the official alcohol tables (part 3), issued by the

The Ministry of Agriculture of the CZECH REPUBLIC, Prague, 1995.



Annex 2



Species and minimum allowances denaturants and purpose of use

denatured alcohol



+-----------+-------------------+-----------------------------+ -------------------------------------------------+

| | | The addition of the undiluted | |

| | | the denaturation of a resource | |

| | +--------------+--------------+ |

| Show. | Denaturing | The smallest | The smallest | Intended use denatured alcohol |

| | | Encore | Encore | |

| | the denaturation denaturation | | | |

| | resource resource | | on | |

| | | 1 l ethanol | 1 m3 of ethanol | |

| | | 20 St. | C | |

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

1A Making 10 ml 10 l not limited

Denaturation of Denatonium 10 mg 10 g

mix for benzoate

in General (Bitrex,

denatured Benzyldiethyl-N-

ethanol 2.6-

-xylylcarbamoyl

methyl-

ammonium

benzoate)

Metylenová blue 2 mg 2 g

Thiophene 2 ml 2 l

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

1B solvent naphtha 4 ml 4 l not limited

Denaturing Kerosene 2 ml 2 l

mix for a technical 1 ml 1 l

in General, gasoline

denatured cleaning

ethanol

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

2 Petrol medical 10 ml 10 ml for laboratory purposes, to use

in medical devices and

pharmacies, to supply to the citizens

pharmacies in packages of up to 200 ml,

the supply to distributors léčiv3) to

production of pectin, for the manufacture of medicinal products, to

production of disinfectants

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

3 Petrol medical 20 ml 20 l to the technical use of all

the kind of outside sales

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

4 Petrol 20 ml 20 l to the technical use of all

technical kind outside sales

cleaning

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

5 Kerosene on 20 ml of 20 l to the technical use of all

light kind off sales

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

6 20 ml 20 ml of Toluene to the technical use of all

the kind of outside sales

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

7 Ajatin 10 g 10 kg to maskérským purposes

(Benzododecinii

bromide)

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

8 Ajatin mixed 100 g 100 kg for the manufacture of cosmetic

with 1,2,3-propanetriol (10 g ajatinu and ajatinu (10 kg and 90 products

90 g glycerol) kg of glycerol)

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

9 Acetone 50 ml 50 ml for the production of fine chemicals,

metal fibres, catalytic converters,

vacuum tubes, tv

screens, semiconductors

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

10 100 ml Acetone 100 l to the technical use of all

the kind of outside sales

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

11 Phenol 4 g 4 kg for hospital purposes, production

photo paper, films and

paper for the production of cork boards,

in the manufacture of gaskets

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

12 10 ml 10 ml Hexane for laboratory purposes


+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

13 2-propanol 100 ml 100 l for the production of fine chemicals,

(Isopropylalk the production of catalysts, to produce

shave) cosmetics, for the preservation of

natural flowers to Kolin

waters

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

14 Methanol 50 ml 50 ml for laboratory purposes

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

15 Shellac 50 g 50 kg for the manufacture of varnishes, glazes, apretur,

politur and mirrors

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

16 Vinegar fermentation 200 ml 200 l to produce fermented distilled vinegar

spirit of the

the concentration of

10%

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

17 etylnatý Acetate 20 g 20 kg to produce acetate, etylnatého, to

adjusting drinking water

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

18 Ammonia 10 ml 10 l to produce feed yeast Torula,

for the manufacture of Diastabil

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

19 30 mg of Denatonium 30 g for the manufacture of cosmetic products,

benzoate which does not come into contact with

(Bitrex, examples

Benzyldiethyl-N-

2.6-

-xylylcarbamoyl

methyl ammonium

benzoate)

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

20 mg of Denatonium 2 2 g for technical use in

Hexyl exclusively for exclusively for processors of ethyl alcohol, which means

(Bitrex, Chrysalis Chrysalis any use outside of the sales and

Benzyldiethyl-N-synthetic synthetic production of products with the

2.6-technical/technical/* alcohol

-xylylcarbamoyl

methyl ammonium

benzoate)

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

21 10 mg of Denatonium 10 g for technical use in

Hexyl exclusively for exclusively for processors of ethyl alcohol, which means

(Bitrex, Chrysalis Chrysalis any use outside of the sales and

Benzyldiethyl-N-fermentation the fermentation production of products with the

2.6-hydrotreated hydrocracked alcohol

-xylylcarbamoyl refined/refined/**

methyl ammonium

benzoate)

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+



22 Motor 20 ml 20 l to produce motor

fuel fuel or ETBE

complying with the

ČSN EN 228



+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

23 Etyltercbuty 20 ml to 20 l for the production of ETBE

lether

(ETBE)

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

24 Metyltercbuty 20 ml 20 l for the production of ETBE

lether (MTBE)

+-----------+-------------------+--------------+--------------+ -------------------------------------------------+

/* the resulting product is a synthetic ethyl alcohol technical a strangely

denatured-see annex 3 of this order

/* the resulting product is oddly denatured alcohol fermentation

hydrotreated-see annex 3 of this order.



Annex 3



Qualitative characters of each species of ethyl alcohol

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Free Nitrogen Extract

Ethanol Methanol in% Higher in acid Fural Aldehydes dried policy when Esters

Vol. in g/la of alcohols in mg/l mg/la as as 105 degrees C in the

At least no more than the kind of alcohol in mg/la no more than a maximum of methylamine acid mg/la la * mg/other characters

up to a maximum not exceeding the acetic

mg/mg/la la * *

up to a maximum of

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Synthetic 95.7 50 50 10 10 25

destilačně

refined

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Synthetic 99.7 250 50 30 benzene and petrol not exceeding 0.1%

anhydrous vol. Dietylester up

0.1% by weight.

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Synthetic 92.9 300 15 25 Dietylester up to 4 g/la.

technical total content of higher alcohols and

other volatile components

at least 5 g/la.

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Sulphite 95.0 40.0 400 500 0.1 40.0

raw

Fermentative raw:

-potato 2.0 80.0 3.0 3500 500 200

-grain 80.0 1.0 5.0 4000 500 200

-starch 80.0 3.0 1.0 3500 500 200

-drožďárenský 85.0 4500 0.01 500 150

-melasový 85.0 0.01 3000 700 300

from 70.0 15.0 6.0 500 5000 800

-beet 80.0 3000 700 5.0 250

-fruit 70.0 15.0 6.0 500 5000 800

waste

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Fermenting smell and taste pure, free of extraneous

refined: odours and flavours, corresponding

-gentle 95.7 0.8 25 1 10 50 35 20 negative processed raw material, the appearance of a clear

-Superfine-96.0 0.0 1 5 10 0 5 30 without the negative of deposit and sedlin **



Smell and taste pure, free of extraneous

-Superfine-96.0 0.3 5.0 5.0 neproka-15 15 13 1.0 odours and flavours, corresponding

neutral zatelný processed raw material, the appearance of a clear

No, the content of deposit and sedlin

tertiary butanol (2-methyl-2-

-technical 95.7 2.4 150 100 50 2 15 OL) maximum negative 5 mg/la *

Appearance clear, without of deposit and

sedlin **

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

The fermentation

anhydrous: appearance clear, without of deposit and

-to 750 30 20 99.8 3.0 sedlin **

industrial

purposes

-the specific 99.7 1.0 60 50 60 10

industrial

purposes

-to

analytical and 99.7 0.1 10 20 10 10

Special

health

purposes

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Fruit and other smell and taste pure, free of extraneous

distillates odours and flavours, corresponding

(a semi-finished product): processed the raw material and the degree of

-borovičkový 37.5 to 70 rectification **

-a pear-shaped 38-75 15 40

-Apple up to 75 15 40 38

-Apricot 75 15 38 to Look clear, without of deposit and

-38 to 75 15 50 Slivovitz sedlin **

-Cherry 38 to 75 15 40

-wine 37.5-75 2 80

-whiskový 40 to 94 15 40

-Peach 38-75 15

-Cherry 38 to 75 15 40

-grain 40 to 94 15 20

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Oddly out of the total content of higher

denatured alcohols, tertiary content

316 25 20 25 790 butanol fermentation of at least 50 mg/la *,

hydrotreated-90 *** 0.39 10 mg of Denatonium benzoate/la *,

the sum of higher alcohols, refined at least

7000 mg/la.


60

-Waterless, clear, free of deposit and sedlin,

the specified maximum water content 99.7 16000 0.3%

a) *** (m/m), the denaturants

motor in the types and quantities of specified

fuels * *** * in Appendix 2 of this order

(b)) for the production in the

ETBE and) 22

(b)) 23 and 24.

The amount of denaturing

the funds may not exceed

the minimum quantity laid down

This decree by more than 50%.

-other 72 *** denaturant in the types of

and quantity specified in the annex

# 2 of this order.

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Oddly the denaturants in the types of

denatured 95.7 *** and the quantity specified in the annex.

synthetic 2 of this order

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Oddly the total content of higher alcohols and

denatured 92.9 *** other volatile components

synthetic at least 7 g/la *, of which at least

technical 4 g/la * sums of all butanolů,

Of denatonium benzoate 2 mg/la *.

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

In General, the denaturant in the types of

denatured and the quantity specified in the annex.

fermentation: 2 of this order.

-92% 92.0 *** 150 250 clear, without of deposit and sedlin,

-95% 95.0 *** 150 250 maximum water content of 0.3% (m/m),

-99.7%, 99.7% *** amount of denaturing

designated funds may not exceed

and) the minimum quantity laid down

motor this decree by more than 50%.

fuels * * * * *

(b)) for the production of

ETBE

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

In General, the

denatured 95.0 ***

synthetic

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Splash 93.1 **** Smell strongly influenced by impurities

Dokapy 88.0 **** from lower and higher bottoms

the factions before or after the separation

ethanol

-------------- ----------------------------------------------------- -------------------------------------------- ------------------------------------

Note:

* la = 1 litre of ethanol concentration of 100% vol.

* rates from the sample after dilution with water at 30% vol.

ethanol and at a temperature of 30-35 degrees C

before adding the denaturation of the resource

does not apply to the production and rectification of fruit and other spirits

the quality must satisfy the ČSN 65 6511.



------------------------------------------------------------ ---------------------------------------- --------------------------------------------

The type of alcohol Ethanol in% of all the higher density of the Mixture of ethanol and water in% of amylalkoholů (a distillate from 110

alcohols in% by volume as the acid at 20 St. vol. up to 135 degrees C) in% vol.

maximum volume at least acetic in mg/la C in kg/m3 at least

up to a maximum of

------------------------------------------------------------ ---------------------------------------- --------------------------------------------

Fusel oil 15 80 500 847 20 45

------------------------------------------------------------ ---------------------------------------- --------------------------------------------



Annex 4



Alcohol loss standards

+----+--------+-----+----------------------+--------------------------+

| Cost | Species | Standard | Specification of activities | The basis for the calculation of the standard |

|-| REF losses | v % | | losses |

| lo | | | | |

+----+--------+-----+----------------------+--------------------------+

| 1 | Traffic | 0,25 | right | amount of alcohol |

| | | | in truck tankers of under and | |

| | | | other tankers | packing slip; to |

| | 2.00 | right | in | base cannot be counted |

| | | | | deliveries under the railway section 8 (2). 2 |

| | | | * | and tanker 3 of this order |

| | 0.30 | right | in metal | |

| | | |-glass tubs | |

| | | ' | ' or other packaging | |

| | | In addition to the wooden | | |

| | 0.60 | right | in wood | |

| | | | barrels | |

+----+--------+-----+----------------------+--------------------------+

| 2 | Han-| | | 0.10 handling in the total intake of alcohol without |

| | Double | | | agricultural and initial stocks and |

| | | | | total Edition fruit distilleries of alcohol without |

| | | | closing stocks | |

| | | | | |

| | | | | for handling 0.10 zemědělský lihovar |

| | | | in agricultural alcohol intake without initial | |

| | | | | supplies and financial support for the refinery |

| | | stand-alone refineries, | | total Edition of alcohol |

| | | If you lead these two | | without closing stocks |

| | | a separate plant | | |

| | | and between the record | | |

| | | There is no plant | | |

| | | transport of ethyl alcohol, | to but | |

| | | | evidenčnímu only | |

| | | alcohol conversion | | |

| | | | | |

| | | 0.05 | manipulation in other total income of alcohol without | |

| | | agricultural and | | than the initial inventory and |

| | | fruit distilleries | | total Edition of alcohol without |

| | | excluding production | end | stocks |

| | | | down | |

| | | | | |

| | | 0.05 | handling in the total quantity of alcohol likérkách | |

| | | | other | contained in products |

| | | | | passed on the processors alcohol warehouse |

| | | | | FG |

+----+--------+-----+----------------------+--------------------------+

| 3 | Bottling | 0.10 | storage of alcohol and registered quantity of alcohol | |

| | in the input | in other preparations | | on the stock manufacturer and |

| | | than wood processor | | and |

| | | containers quantity registered | | alcohol |

| | | | inventory of State | |

| | | | | material reserves |

| | | | | 0.20 storage preparations to the last day |

| | | in wooden containers | | calendar month |

| | | more than content | | | base with

| | | ' | ' is not allowed to 300 liters | |

| | | | count toward the stocks of ethyl alcohol and | |

| | | | | 0.35 storage preparations the quantity of alcohol in the finished |

| | | in wooden containers | | rolled products |

| | | | | not more than to dispatch or |

| | | 300 litres | | consumer packaging |

+----+--------+-----+----------------------+--------------------------+

| 4 | Bottling | 0.60 | racking emulsion quantity of alcohol contained | |

| | | liquors of all kinds | | in the twisted products |

| | | packing, decanting | | transmitted on uk |

| | | | other spirits and other spirituous beverages and | |

| | | | other | processors alcohol |

| | | containing alcohol to | | |

| | | packaging of smaller content | | |

| | | than 0.1 litre | | |

| | | | | |

| | 0.45 bottling of potable | | | |

| | | ethyl alcohol, of spirituous beverages | other | |

| | | |-containing products | |

| | | alcohol, packaged | content | |

| | | from 0.1 to 0.35 | l | |

| | | | except emulsion | |

| | | | liqueurs | |

| | | | | |

| | 0.35 bottling of potable | | | |

| | | alcohol, spirits | | |

| | | ' | ' and other products | |

| | | containing alcohol to | | |

| | | packages larger than 0.35 | | |

| | | | l | |

| | | | except emulsion | |

| | | | liqueurs | |

+----+--------+-----+----------------------+--------------------------+

| 5 | When refining the fermentation 1.10 | | | amount of fermented |

| | editing | the raw alcohol, | | raw ethyl alcohol, used |

| | alcohol | | except | for refining |

| | | | drožďárenského alcohol | |

| | | | | |


| | | | fermented refining 4.00 | amount of fermented |

| | | raw raw drožďárenského | | |

| | | | drožďárenského ethyl alcohol used to ethyl alcohol, | |

| | | | |-refining |

| | | | | |

| | | | refining 2.50 spills and spills and quantity dokapů |, |

| | | | dokapů | used for refining |

| | | | | |

| | | | the amount of alcohol used to ' | ' |

| | | 1.50 | alcohol dehydration | drainage |

| | | | | |

| | | | | 8.00 alcohol dehydration quantity of ethyl alcohol used to |

| | | | | |-based MERCK drainage

| | | | | |

| | | | 1.30 rectification of fruit and the quantity of alcohol in the raw | |

| | | | other distillates the distillate during separate | |

| | | | rectification or quantity | |

| | | | alcohol in the distillate at | |

| | | | the second rectification ** | |

| | | | | |

| | | | regeneration of ethyl alcohol from 1.00 | amount of ethyl alcohol contained |

| | | | | substances containing ethyl alcohol substances used to |

| | | | alcohol recovery | ** |

+----+--------+-----+----------------------+--------------------------+

| 6 | When the production macerátů 3.60 | | |, the total consumption of alcohol |

| |-OCC | | | used to manufacture |

| | tion | | | macerátů |

| | alcohol | | | |

| | | průtahových | 1.30 | alcohol production quantity used |

| | | | | in the production of spirits of swipe |

| | | | | distillate |

| | | | | |

| | | 3.00 | storage of spirits and quantities of spirit drinks and | |

| | | fruit and other | | fruit and other |

| | | spirits (semi-finished) | | spirits (semi-finished products) |

| | | | other physical | according to those that were |

| | | | or chemical | fixed |

| | | | or | routing methods |

| | | | vymrazováním | done artificial storage |

| | | | When any of the physical | |

| | | | vymrazený | or separated by chemical methods |

| | | | | share or in which the |

| | | | technological | made |

| | | | Edit by freeze drying | |

| | | | | fixed |

| | | | | Routing |

| | | | with the subsequent Department | |

| | | | | vymrazeného share |

| | | | | |

| | | | 1.80 malt whisky production quantity of ethyl alcohol contained | |

| | | | the stock specified with | |

| | | | | to produce malt whisky |

| | | | | |

| | | | potable alcohol 0.90 production quantities of alcohol used, | |

| | | | 80% | to produce semi-finished product |

| | | | potable alcohol 80% | | |

| | | | | |

| | | | alcohol filtration over 1.00 | amount of alcohol used |

| | | | | activated carbon, to perform technology |

| | | | karbonifikace and other specified adjustment procedure | |

| | | physical or alcohol | | one of |

| | | chemical treatment of alcohol | | specified methods |

| | | | | |

| | | | alcohol bentonite flocculation 3.60 | quantity of alcohol for which |

| | | with the subsequent filtration | | according to technological |

| | | | the procedure made clarification | |

| | | | bentonite with subsequent | |

| | | | | filtration |

| | | | | |

| | | | | 0.30 mending of spirits amount of ethyl alcohol contained |

| | | | | in spirits which |

| | | | ' | ' was made |

| | | | | technological |

| | | | | levelness coupage |

| | | | different spirits | |

| | | | | |

| | | | | 1.60 emulsion production quantities of alcohol used |

| | | | | for the manufacture of liquors, liqueurs emulsion |

| | | | | |



| | production of spirits 1.00 | | | amount of alcohol used |

| | | | except for the production of spirits, | |

| | | | |, except liqueurs emulsion emulsion |

| | | | & manufacture of other liqueurs, and quantity | alcohol |

| | | | |-containing products used in the manufacture of other |

| | | including the production of alcohol | | products containing alcohol |

| | | | motor fuels | |

+----+--------+-----+----------------------+--------------------------+



Note:

* For losses to the standards by the losses

occurred in the transportation of alcohol by rail in rail tankers,

not more than 2%, if these losses

There was, in the circumstances specified in article 2(1). 31 Uniform

legislation for the Treaty on the international

the carriage of goods by rail (CIM-Hook (B)

to the Convention), as amended by notice No. 49/2006 Coll. m. s., the Decree

No. 8/1985 Coll., on the Convention on international rail

carriage by rail (COTIF), as amended

regulations, and under the condition that a railway tank wagon,

that loss was detected, was on all vpustních

výpustních holes and secure seals.

** The use of standards is bound to allow the Ministry of Finance according to the

§ 8 para. 1 of the law.

The use of standards is subject to the authorisation by the Ministry of finance

§ 8 para. 3 of the Act.



ČSN 73 0804 1) fire safety of buildings-industrial buildings.



1A) of section 9 of Act No. 505/1990 Coll. on metrology.



1A) Act 353/2003 Coll., on the Excise Tax Act, as amended

regulations.



1B) Act 505/1990 Coll., on metrology, as amended.



2) Decree No. 150/2008 Coll., on the control of the production and circulation of ethyl alcohol and

the implementation of other provisions of the law on alcohol related.



3) Act 79/1997 Coll., on pharmaceuticals and on amendments and additions to some

related laws, as amended.